Re: Decomposition test

From: Douglas L. Marshall (DMarshall@foodscience.msstate.edu)
Date: Fri Mar 30 2007 - 12:50:20 PDT

  • Next message: Rippen, Thomas E.: "RE: Decomposition test"

    For those who may be interested we've published a few papers on the
    topic using a very simple impedimetric test. For details see....

    Wiese-Lehigh, P.L. and D.L. Marshall. 1993. Determination of seafood
    freshness using impedance technology. In Food Flavor & Safety:
    Molecular Analysis and Design. A.M. Spanier, H. Okai, and M. Tamura
    (Eds.). ACS Symposium Series No. 528, American Chemical Society,
    Washington, D.C., Chapter 20, pp. 248-261.

    Marshall, D.L. and P.L.W. Lehigh. 1993. Nobody's nose knows.
    CHEMTECH 23:38-42.

    Marshall, D.L. and P.L.W. Lehigh. 1997. Comparison of impedance,
    microbial, sensory, and pH methods to determine shrimp quality. Journal
    of Aquatic Food Product Technology 6(2):17-31.

    Cotton, L.N. and D.L. Marshall. 1998. Rapid impediometric method to
    determine crustacean food freshness. In New Techniques in the Analysis
    of Foods. M.H. Tunick, S.A. Palumbo, and P.M. Fratamico (Eds.). Plenum
    Publishing Corp., New York, Chapter 13, pp. 147-160.

    Bazemore, R., S.G. Fu, Y. Yoon, and D. Marshall. 2003. Major causes
    of shrimp spoilage and methods for assessment. In Off-Flavors in
    Aquaculture. A.M. Rimando and K.K. Schrader (Eds.). ACS Symposium
    Series No. 848, American Chemical Society, Washington, D.C., Chapter 16,
    pp. 223-234.

    Metcalfe, A.M. and D.L. Marshall. 2004. Capacitance method to
    determine the microbiological quality of raw shrimp (Penaeus setiferus).
     Food Microbiology 21:361-364.

    *************************************************
    Douglas L. Marshall, Ph.D.
    Professor, Mississippi State University
    Department of Food Science, Nutrition, & Health Promotion
    Room 160A Herzer, Stone Blvd. (courier)
    Box 9805 (post)
    Mississippi State, MS 39762-9805
    1-662-325-8722 (voice)
    1-662-325-8728 (fax)
    microman@ra.msstate.edu (email)
    http://www.msstate.edu/dept/fsnhp
    *************************************************

    >>> "P Howgate" <phowgate@clara.co.uk> 03/30/07 2:27 PM >>>
    I would like to support Hector Lupin's recent comments on the topic of

    sensory and non-sensory evaluation of spoilage and add a few comments
    of my
    own. In my many years of experience of meeting quality controllers in
    processing plants, discussing quality control with quality controllers

    elsewhere, and discussing with other people interested in quality
    control in
    industry I never came across, or heard of, any examples of non-sensory
    tests
    being used in quality control of fish or fishery products in industry
    for
    evaluation of freshness/spoilage other than to meet possible
    requirements of
    regulatory agencies or if required by customers. And examples would be

    analysis for indole in shrimp to meet US import requirements when these
    were
    in force. There is very little information about chemical spoilage
    indicators in crab meat and I am not aware of any proposed criteria for
    any
    chemical tests. Though indole has been suggested as an indicator of
    spoilage
    for shrimp and prawns it has not been demonstrated to be an effective
    index.
    There used to be US guidelines for indole in shrimp, but I think these
    have
    been discontinued, though someone closer to the scene can confirm this,
    or
    not. There is an excellent review of indole in shrimp and prawns,
    including
    regulatory aspects, in Oehlenschläger, J. & Luten, J.B. (2005), Review:

    Indole as a quality indicator in shrimps and prawns, Archiv für
    Lebensmittelhygiene, 56, 52-57.

    Studies on TVB as an indicator of spoilage started about 90 years ago,
    but
    it is not an effective chemical index for spoilage in fish despite its

    inclusion in EU regulations. Studies and TMA as a measure of spoilage
    date
    from about 80 years ago and though this is a little better than TVB as
    an
    index of spoilage it is still not nearly good enough and I am not aware
    of
    its inclusion in any regulatory requirements. It is certainly of no
    value
    for in-line quality control in industry.

    I can not allow Klaus Schallié's comments about the difficulties of
    using
    sensory evaluation in industrial situations to go unchallenged in case
    it
    puts people off using the technique. Though now retired when I was
    active I
    had considerable experience of sensory evaluation of fish and fishery
    products in both the research and the industrial situations, though
    mostly
    the former. I was involved in a study of the feasibility and accuracy
    of
    sensory evaluation of raw fish at port markets and there was no
    suggestion
    that the assessors were any less accurate at the port markets than they
    were
    in the laboratory. Though the possible distractions that Klaus might be

    present in a particular situation the purpose of training is to ensure
    that
    the assessors can ignore these and give an accurate and precise
    evaluation
    of the sensory properties of the product under examination. There is no

    foundation in believing that the assessors would be accurate only with
    poor
    quality fish. My experience of quality control in fish processing
    plants in
    Britain that operated to good quality assurance protocols was that they

    relied entirely on sensory procedures for their quality control and
    quality
    assurance, and that was for control limit equivalent to freshness of
    fish
    four days in ice for demersal fish or for frozen fish showing no, or
    only
    negligible, signs of cold storage change. On one occasion I had a group
    of
    quality controllers from a processing plant visit my laboratory for
    collaboration with the laboratory panel. They told me that in a working

    shift they would assess all batches of fish entering the process by
    evaluation in the raw state and during processing samples were
    frequently
    taken from the processing lines and evaluated after cooking. They had a
    test
    kitchen, but that was not fitted out as a centre evaluation facility as

    would be found in research institutes. They told me that they evaluated

    somewhere in the order of 70 cooked samples a shift. I didn't make any

    statistical checks on the performance of the quality controllers
    compared
    with my laboratory panel, but with that degree of experience on a daily

    basis I had a sneaking feeling that they would be better than my
    panel.

    I do not understand why people are so afraid of sensory evaluation and
    wish
    to find a chemical substitute. All chemical tests have to be calibrated

    against sensory evaluation if they are to prove their worth and none
    can be
    any better than sensory evaluation. Chemical tests are more costly to
    carry
    out and more time-consuming than sensory evaluation and will always be

    considered inferior and unreliable substitutes for it. True there is
    some
    overheads in selecting and training quality controllers in sensory
    evaluation, but after that there is little extra cost to the company
    because
    they are employing the quality controllers anyway. Don't forget that
    sensory
    evaluation can detect defects that will be missed by chemical tests,
    for
    example taints, and is much closer to the way consumers evaluate the
    quality
    of the product.

    Peter Howgate

    ----- Original Message -----
    From: "Surefish Bellingham" <Surefish@az.com>
    To: <seafood@ucdavis.edu>
    Sent: Thursday, March 29, 2007 4:53 PM
    Subject: Decomposition test

    Is there any rapid test (other than sensory) for decomposition on a raw

    product?

    Thanks,

    Mark Neely
    Surefish, Inc.



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