Re: Total Volatile Bases in Fish

From: Howgate (phowgate@rsc.co.uk)
Date: Thu Oct 19 2000 - 12:12:29 PDT

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    Dear Tim and Listers

    In response to the query by Tim Koester on TVB.

    I attach as a file that part of lecture notes of mine on chemical methods
    for measuring freshness of fish dealing with TVB. The file is in .rtf format
    so should be readable in any word processor. Bearing in mind Pamela's recent
    comment on viruses, I have Norton antivirus software installed on my system.

    There is a very large literature on TVB in fish, probably 3-400 references
    make some reference. It has been applied to a very large variety of fish
    species, vertebrate and invertebrate. Apart from the distillation procedures
    summarised in my notes, methods based on other principles have been
    described claiming some advantage over the simple distillation ones. Despite
    all this effort, TVB is, and always will be, a very poor indicator of
    freshness of fish. I can not be used reliably for quality assurance of fish
    products for retail sale. TVB does not increase until the fish is past its
    good quality condition and near its unfit for consumption stage. It is
    included in an EU Directive, but in my opinion that inclusion could only
    have been a political decision rather than one based on its merit -
    hypoxanthine or inosine monophosphate contents, or K value are much better.
    Try the following references for studies on reliability of TVB measurement,
    and brief, but good, reviews - by Oehlenschläger - of its application and
    limitations.

    Peter Howgate

    Antonacopoulos, N. & Vyncke, W. (1989). Determination of volatile basic
    nitrogen: a third collaborative study by the West European Fish
    Technologists' Association (WEFTA). Zeitschrift für
    Lebensmittel-Untersuchung und -Forschung, 189, 309-316

    Oehlenschläger, J. (1992). Evaluation of some well established and some
    underrated indices for the determination of freshness and/or spoilage of ice
    stored wet fish. In: Quality Assurance in the Fish Industry, H.H. Huss, M.
    Jakobsen & J. Liston, eds, Elsevier Science Publishers, Amsterdam, pp
    339-350. ISBN 0 444 89077-7

    Oehlenschläger, J. (1992). Suitability of ammonia, dimethylamine,
    trimethylamine, trimethylamine oxide and TVB as freshness indicators in
    seafoods. In: Methods to determine the freshness of fish in research and
    industry. Proceedings of the final meeting of the concerted action"
    Evaluation of fish freshness" AIR3CT94 2283. (Edited by Ólafsdóttir, G.,
    Luten, J., Dalgaard, P. Careche, M. Verrez-Bagnis, V. Martinsdottir, E. &
    Heia, K.). Pp92-99. International Institute of Refrigeration, Paris. ISBN
    2-9033633959.

    Vyncke, W. (1996). Comparison of the official EC method for the
    determination of total volatile bases in fish with routine methods. Archiv
    für Lebensmittelhygiene, 47, 110-112

    Vyncke, W., Luten, J., Brünner, K. & Moermans, R. (1987). Determination of
    total volatile bases in fish: a collaborative study by the West European
    Fish Technologists ' Association (WEFTA). Zeitschrift für
    Lebensmittel-Untersuchung und -Forschung, 184, 110-114





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